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This book discusses the efficacy of nanomaterial-based X-rays enhancers against cancer therapy and imaging in both in vitro and in vivo systems. Also, synthesis, mechanism, and the related biological effects are given. Moreover, nanoparticle-based contrast agents to enhance the image quality are compiled. Finally, special nanoparticle-based contrast agents to enhance the contrast for targeted cancer therapy are covered and discussed. X-rays Based Bioimaging Techniques and Scintillating Materials Radiosensitizers in Radiation-Induced Cancer Therapy Emerging Nanomaterials as Radio-Sensitizer in Radiotherapy Nanoradiosensitzers: Preparation, Characterization and Their Performance Harnessing the Power of Nanomaterials to Alleviate Tumor Hypoxia in Favor of Cancer Therapy Application of Nanoradioprotective Agents in Cancer Therapy X-ray Triggered Photodynamic Therapy Nanoparticle Based CT Contrast Agents Natural Radioprotectors ROS-Based Cancer Radiotherapy